UNDERGROUND STORAGE TANKS

Parameter

Method

Detector

  

BTEX

8260B

MS

BTEX

602/8021B

PID

BTEX plus MTBE

602/8021B

PID

BTEX plus Naphthalene

602/8021B

PID

Diesel Range Organics (C12-C24)

8015B

Extraction – FID

Gasoline Range Organics (GRO/C5-C12)

8015B

Purge - FID

Polynuclear Aromatic HCs (PAHs or PNAs)

8270C

MS

TPH-DRO

see Diesel Range Organics

FID

TPH-GRO

see Gasoline Range Organics

FID

TPH-EPH

TN Method

FID

TPH-GRO

TN Method

FID

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 HAZARDOUS WASTE CHARACTERIZATION

 

Parameter

Method

 

Reactivity (cyanide & sulfide)

7.3.3.2/7.3.4.2 9010/0934

Corrosivity (pH)

9040B/9045C

Ignitability

1010

Toxicity (TCLP)

 

           Metals (8)

Various

           Volatile Organics

8260B

           Semivolatile Organics

8270C

           Pesticides

8081A

           Herbicides

8151A

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TCLP

 

 

Parameter

Method

 

Toxicity (TCLP

 

           Metals (8)

Various

           Volatile Organics

8260B

           Semivolatile Organics

8270C

           Pesticides

8081A

           Herbicides

8151A

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  NPDES (Priority Pollutants)

 

Parameter

Method

 

Volatile Organics

624

Semivolatile Organics (ABNs)

625

         Acid Extractable Organics

625

         Base Neutral Extractable Organics

625

Pesticides and PCBs

608

Metals (13)

Various

Phenolics & Cyanide

420.1&335.4

Radiological (Subcontracted)

 

Dioxin (Subcontracted)

 

 

For Form 2C, Form 2P, Repermitting or similar Permit Applications, call to

 

confirm requirements.  Individual quotations will be prepared based on

 

the required testing and detection limits.

 

 

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  TARGET ANALYTE  and TARGET COMPOUND LIST

 

Parameter

Method

 

TAL - 23 Metals (23) plus Cyanide

Various

TCL - Volatiles Organics

8260B

TCL - Semivolatiles Organics (ABNs)

8270C

TCL – Pesticides and PCBs

8081A/8082

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   BROWNFIELD (partial listing only - call for further information)

 

Parameter

Method

Detector

 

EPH

MA Method

FID

VPH

MA Method

PID

Moisture          Required for EPH & VPH

160.3

 

PAHs               Acceptable for soil

8270C

MS

PAHs               Required for water

8310

HPLC

Volatile Organics (67)

8260B

 MS

Semivolatile Organics (78)

8270C

MS

Pesticides/PCBs (27)

8081A/8082

ECD

Herbicides (3)

8151A

ECD

Metals (28)     (metal compounds are not reported)

Various

 

 

Note: the value in parenthesis indicates the number of reported parameters.

Laboratories typically cannot analyze for all the compounds listed in the Tier 1

TRG Table.   Please contact Client Services for further details.

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  APPENDIX I (water)

Parameter

Method

 

Metals (15)

Various

Volatile Organics

8260B

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  APPENDIX II (water)

Parameter

Method

 

Inorganics (17 Metals + Cyanide & Sulfide)

Various

Volatile Organics

8260B

Semivolatile Organics (ABNs)

8270C

Pesticides and PCBs

8081A/8082

Organophosphorus Pesticides

8141A

Herbicides

8151A

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  APPENDIX IX (soil)

Parameter

Method

 

Inorganics (17 Metals + Cyanide & Sulfide)

Various

Volatile Organics

8260B

Semivolatile Organics (ABNs)

8270C

Pesticides and PCBs

8081A/8082

Organophosphorus Pesticides

8141A

Herbicides

8151A

Dioxins & Furans (Subcontracted)

8290

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  F001-005 (solvents)

 

Parameter

Method

 

Volatiles

8260B

Semivolatiles

8270C

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   F039 (solvents)

Parameter

Method

 

Herbicides

8151A

Pesticides and PCBs

8081A/8082

Semivolatile Organics (ABNs)

8270C

Volatile Organics

8260B

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   BIOSOLIDS (EPA Part 503)

 

Parameter

Method

 

Fecal Coliform (MPN) (see note)     requires % solids

9221E

Fecal Coliform (see note) requires % solids

9222D

Metals (10) requires % solids

Various

Solids (%)

2540G

SOUR

2710B

 

Note: For municipalities, the EPA and the State of Mississippi prefer and

highly recommend method 9221E (tube).  Method 9222D (MF) is not

recommended.  Also, to assure proper sampling, a geometric mean should be

reported from seven random samples.

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   FISH TISSUE

Parameter

Method

Detector

 

Antibiotics

 

HPLC

MS Pesticide Scan

 

ECD, NPD, & HPLC

Fat %

3.003

 

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   DRINKING WATER (call Client Services to confirm parameters)

Parameter

Method

Detector

 

Bacteriological - Total Coliform

MMO-MUG Colilert

 

Chemical

Call for parameter listing

 

Inorganics

Call for parameter listing

 

Lead and Copper

200.9

 

Radiological (Subcontracted)

 

 

        Radium 226

 

 

        Alpha emitters and Beta-particle

 

 

        Photon emitters

 

 

        Radon, Radium -228, Uranium

 

 

Secondary Contaminants

Call for parameter listing

 

Unregulated Contaminants

Call for parameter listing

 

Diquat & Paraquat

549.1

HPLC - DAD

Endothall

548.1

ECD

Glyphosphate

547

HPLC - Fl

Herbicides

515.1

ECD

Pesticides and PCBs

508

ECD

Carbamates

531.1

HPLC - Fl

Organophosphates

507

NPD

Trihalomethanes

524.2

MS

Volatile Organics

524.2

MS

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   MICROBIOLOGY (water matrix)

Parameter

Method

 

Bacteria, Total

9215B

Clostridium perfringens

BBL

Coliforms, Fecal

9222D

Coliforms, Total

Colilert

Fecal Coliform    (MPN)    (includes TS)

9221E (tube)

E. coli

1103.1

Gram Stain

 

Legionella

BBL

Pseudomonas aeruginosa

BBL

Salmonella

9260D

Standard Plate Count

9215B

Staphylococcus aureus

9213B

Streptococcus, Fecal

9230C

Yeast and Molds

9610B

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  INDUSTRIAL HYGIENE (Air Matrix)

 

Parameter

Method

 

Alcohols

NIOSH 1400

Aromatic Hydrocarbons (BTEX)

NIOSH 1501

Formaldehyde

NIOSH 3500

Ketones

NIOSH 1300

Methylene Chloride

NIOSH 1005

Methyl ethyl ketone

NIOSH 2500

Solvent Scan

Various

Welding fume metals (13)

Various

 

OVMs and other sampling media - call for further information.

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  POULTRY

 

Parameter

Method

 

E.coli

Call to set up Project

Moisture

 

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  OIL/FUEL TESTING

 

Parameter

Method

 

Cetane Index (Subcontracted)

D 976

Color

 

Flash Point

1010

Halogens, Total (chlorine) (Subcontracted)

9253

Metals in Oil (As, Cd, Cr, Pb)

D 4928

Moisture (Karl Fischer) (Subcontracted)

D 2216

Moisture (%)

 

PCBs

 

Sulfur (Subcontracted)

D1552 (oil) D 4794 (fuel)

Viscosity (subcontracted)

D 445

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  EXPLOSIVES

 

Parameter

Method

Detector

 

Nitroaromatics & Nitroamines

8330

HPLC - UV

Nitroglycerine

8332

HPLC - UV

Tetrazene

8331

HPLC - UV

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